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    Influence of residual stresses on the crack initiation and short crack propagation in a martensitic spring steel
    The crack initiation and short crack propagation in a martensitic spring steel were investigated by means of in-situ fatigue testing. Shot peened samples as well as untreated samples were exposed to uniaxial alternating stress to analyze the impact of compressive residual stresses. The early fatigue damage started in both sample conditions with the formation of slip bands, which subsequently served as crack initiation sites. Most of the slip bands and, correspondingly, most of the short fatigue cracks initiated at or close to prior austenite grain boundaries. The observed crack density of the emerging network of short cracks increased with the number of cycles and with increasing applied stress amplitudes. Furthermore, the prior austenite grain boundaries acted as obstacles to short crack propagation in both sample conditions. Compressive residual stresses enhanced the fatigue strength, and it is assumed that this beneficial effect was due to a delayed transition from short crack propagation to long crack propagation and a shift of the crack initiation site from the sample surface to the sample interior.
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      2  18
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    On the low temperature creep controlling mechanism in a high strength spring steel
    Despite of the well-known fact that high strength steels are exhibiting low temperature creep deformation, its rate controlling mechanism is yet to be understood. The strain hardening theory and the exhaustion creep model were proposed almost seven decades ago to unravel the low temperature creep mechanism in a single phase homogeneous isotropic material. However, their applicability to low temperature creep deformation in a technical material like a modern high strength steel is still a matter of investigation owing to their nature of multi-phase, in-homogeneous, and an-isotropic behavior. The authors have grabbed this chance to experimentally validate the exhaustion creep model based on low temperature creep tests of the SAE 9254 spring steel.
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      297  173
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    The impact of additive manufacturing on the mechanical properties of a stainless precipitation hardening steel
    A stainless precipitation hardening steel has been qualified for powder bed fusion of metals using a laser beam. The mechanical and microstructural properties of additively manufactured samples have been thoroughly investigated and compared to samples of the very same material made by means of ingot casting. Additive manufacturing is feasible and can deliver superior mechanical properties. Additionally, the surface quality will be improved by means of wet abrasive jet machining, and its impact on the residual stresses has been shown.
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      3  14
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    X-ray diffraction with micrometre spatial resolution for highly absorbing samples
    X-ray diffraction with high spatial resolution is commonly used to characterize (poly)crystalline samples with, for example, respect to local strain, residual stress, grain boundaries and texture. However, the investigation of highly absorbing samples or the simultaneous assessment of high-Z materials by X-ray fluorescence have been limited due to the utilization of low photon energies. Here, a goniometer-based setup implemented at the P06 beamline of PETRA III that allows for micrometre spatial resolution with a photon energy of 35 keV and above is reported. A highly focused beam was achieved by using compound refractive lenses, and high-precision sample manipulation was enabled by a goniometer that allows up to 5D scans (three rotations and two translations). As experimental examples, the determination of local strain variations in martensitic steel samples with micrometre spatial resolution, as well as the simultaneous elemental distribution for high-Z materials in a thin-film solar cell, are demonstrated. The proposed approach allows users from the materialsscience community to determine micro-structural properties even in highly absorbing samples.
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      3  10